Synthesis and Characterization of Heteroleptic Copper(I) and Silver(I) Complexes with Fluorinated Bipyridine and Phenanthroline Ligands

Event Type

Research Presentation

Academic Department

Chemistry

Location

Dana Science Building, 2nd floor

Start Date

24-4-2026 1:00 PM

End Date

24-4-2026 2:30 PM

Description

Organic light emitting diodes (OLED) have shown significant promise as cost effective alternatives to their inorganic counterparts. Within the OLED field, there is currently an effort to replace iridium(III) sensitizers with cheaper and more earth abundant copper(I) and silver(I) alternatives. One issue that needs to be overcome is the pseudo Jahn-Teller distortion in copper(I) complexes, a major quenching pathway. In homoleptic complexes, it has been shown that sterically bulky ligands can be utilized to control Jahn-Teller distortion, resulting in longer emission lifetimes and higher quantum yields. This work aims to use Heteroleptic copper(I) and silver(I) complexes that contain strongly electron-withdrawing and sterically bulky trifluoromethyl groups as a way to tune the fluorescence of the complexes. Preliminary characterization of these compounds was completed with mass spectrometry and single crystal X-ray crystallography (SC-XRD). Heteroleptic structures for several compounds have been confirmed with SC-XRD, while others are still in progress. Additionally, the absorbance and fluorescence properties of the compounds were studied as films and in dichloromethane solutions.

Comments

Under the direction of Dr. Brian Reeves.

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Apr 24th, 1:00 PM Apr 24th, 2:30 PM

Synthesis and Characterization of Heteroleptic Copper(I) and Silver(I) Complexes with Fluorinated Bipyridine and Phenanthroline Ligands

Dana Science Building, 2nd floor

Organic light emitting diodes (OLED) have shown significant promise as cost effective alternatives to their inorganic counterparts. Within the OLED field, there is currently an effort to replace iridium(III) sensitizers with cheaper and more earth abundant copper(I) and silver(I) alternatives. One issue that needs to be overcome is the pseudo Jahn-Teller distortion in copper(I) complexes, a major quenching pathway. In homoleptic complexes, it has been shown that sterically bulky ligands can be utilized to control Jahn-Teller distortion, resulting in longer emission lifetimes and higher quantum yields. This work aims to use Heteroleptic copper(I) and silver(I) complexes that contain strongly electron-withdrawing and sterically bulky trifluoromethyl groups as a way to tune the fluorescence of the complexes. Preliminary characterization of these compounds was completed with mass spectrometry and single crystal X-ray crystallography (SC-XRD). Heteroleptic structures for several compounds have been confirmed with SC-XRD, while others are still in progress. Additionally, the absorbance and fluorescence properties of the compounds were studied as films and in dichloromethane solutions.